Freeze Granulation – Spray Freeze Drying

References

Markets

PowderPro has sold equipment and services for freeze granulation to companies, institutes and universities world wide since 2000. Representation in China, India, Japan, Korea, and USA. Typical applications are for granulation of ceramic powders; oxides (Al2O3, ZrO2, SiO2), nitrides (Si3N4) and carbides (SiC) and also metal oxides, nanopowders, diamonds/CBN, explosives (igniters, delay elements) and for drying of pharmaceuticals and drygs and for drying of biomaterials like proteins and enzymes and fine chemicals.

Scientific papers

Listed below are some scientific papers from PowderPro and Swedish Ceramic Institute showing the benefits with freeze granulation for the manufacturing of engineering ceramics.

    • Improving Powders with Freeze Granulation, Ceramic Industry, April, 40-44, 2003.
    • Si3N4 Powders Applied for Water-Based DCT, Ceramic Transaction 142, 44-62, 2003.
    • Development of Water-Based Processing of Silicon Nitride Materials, Ceram. Eng. Sci. Proc., 23 (3) 3-10, 2002.
    • The Influence of the Granule Structure on the Strength of Pressed and Sintered Si3N4, Sixth ECerS Conf., Ext. Abs. Vol. 2, 1999.
    • Freeze-Granulation of Liquid Phase Sintered Silicon Carbide, Ceramic Transactions 42, 1994.
    • Granulation of Ceramic Powders for Pressing by Spray-Freezing and Freeze-Drying, Euro-Ceramics II, Vol. 1, 1993.

Papers – Download

Improving Powders with Freeze Granulation

Si3N4 powders applied for water-based DCT 

Development of water-based processing of silicon nitride materials

The influence of the granule structure on the strength of pressed and sintrered Si3N4

Freeze granulation of liquid phase sintered silicon carbide

Granulation of ceramic powders for pressing by spray-freeze and freeze-drying

Pressing and sintering developments of Freeze Granulated Si3N4 material

Prospects of Al2O3 and MgAl2O 4-supported CuO oxygen carriers in chemical-looping combustion (CLC) and chemical-looping with oxygen uncoupling (CLOU)